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アプリケーションデータ
Application Data
2L-ChiralTLC®を用いた条件検討
2L-ChiralTLC®IA
- Warfarin Sodium
-
Plate size: 10mm×100mm
Solvent：
n-Hex./IPA/TFA=50/50/0.1
(v/v/v)
Sample conc.: 50,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
- N-CBZ-DL-Valine
-
Plate size: 10mm×100mm
Solvent：
n-Hex./IPA/TFA=70/30/0.1
(v/v/v)
Sample conc.: 100,000ppm in
Eluent
Inj. : 1µL.
Detect：Phosphomolybdic
acid
- Flavanone
-
Plate size: 10mm×100mm
Solvent：n-Hex./EtOAc=90/10
(v/v)
Sample conc.: 5,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
2L-ChiralTLC®IC
- 4-Benzoyloxy-2-azetidinone
-
Plate size: 10mm×100mm
Solvent：
n-Hex./IPA=50/50
(v/v)
Sample conc.: 100,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
- Pindolol
-
Plate size: 10mm×100mm
Solvent：
n-Hex./IPA/DEA=70/30/0.1
(v/v/v)
Sample conc.: 10,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
- 1,5-dihydroxy-1,2,3,4-
tetrahydronaphthalene -
Plate size: 10mm×100mm
Solvent：
DCM/MeOH/AcOH=100/0.1/0.1
(v/v/v)
Sample conc.: 50,000ppm in
Eluent
Inj. : 1µL.
Detect：Iodine
2L-ChiralTLC®ID
- Flavanone
-
Plate size: 10mm×100mm
Solvent：MeOH=100(v)
Sample conc.: 5,000ppm in Eluent
Inj. : 1µL.
Detect：UV254nm
- Aminoglutethimide
-
Plate size: 10mm×100mm
Solvent：EtOAc/DEA=100/0.1
(v/v)
Sample conc.: 50,000ppm in Eluent
Inj. : 1µL.
Detect：UV254nm
2L-ChiralTLC®IF
- Tröger's base
-
Plate size: 10mm×100mm
Solvent：MeOH=100(v)
Sample conc.: 10,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
- Furoin
-
Plate size: 10mm×100mm
Solvent：
n-Hex./EtOH/MeOH=30/40/40
(v/v/v)
Sample conc.: 50,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
- Methyclothiazide
-
Plate size: 10mm×100mm
Solvent：
n-Hex./EtOH/DEA=50/50/0.1
(v/v)
Sample conc.: 10,000ppm in
Eluent
Inj. : 1µL.
Detect：UV254nm
